Information card for entry 4130896

Structure parameters

• Formula: C81 H127 Ge N3 Si2
• Calculated formula: C81.5 H127.35 Ge N3 Si2
• Title of publication: Regiodiscriminating Reactivity of Isolable NHC-Coordinated Disilenyl Germylene and Its Cyclic Isomer.
• Authors of publication: Nieder, David; Huch, Volker; Yildiz, Cem B.; Scheschkewitz, David
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 42
• Pages of publication: 13996 - 14005
• a: 13.255 ± 0.0005 Å
• b: 25.4218 ± 0.0008 Å
• c: 23.768 ± 0.0008 Å
• α: 90°
• β: 101.111 ± 0.002°
• γ: 90°
• Cell volume: 7858.9 ± 0.5 ų
• Cell temperature: 152 ± 2 K
• Ambient diffraction temperature: 152 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0723
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.1323
• Weighted residual factors for all reflections included in the refinement: 0.143
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No