Crystallography Open Database

Information card for entry 4131017

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Coordinates	4131017.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C132 H115 Ag6 Cu F6 P6
Calculated formula	C132 H103 Ag6 Cu F6 P6
Title of publication	Assembly of Heterometallic Silver(I)-Copper(I) Alkyl-1,3-diynyl Clusters via Inner-Core Expansion.
Authors of publication	Hau, Sam C. K.; Yeung, Margaret C.-L.; Yam, Vivian W.-W.; Mak, Thomas C. W.
Journal of publication	Journal of the American Chemical Society
Year of publication	2016
Journal volume	138
Journal issue	41
Pages of publication	13732 - 13739
a	17.2502 ± 0.0014 Å
b	17.4681 ± 0.0014 Å
c	22.3312 ± 0.0018 Å
α	110.625 ± 0.002°
β	103.643 ± 0.002°
γ	94.745 ± 0.002°
Cell volume	6017.5 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1039
Residual factor for significantly intense reflections	0.0874
Weighted residual factors for significantly intense reflections	0.235
Weighted residual factors for all reflections included in the refinement	0.2597
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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