Information card for entry 4131179

Structure parameters

• Formula: C44 H70 N4 P V
• Calculated formula: C44 H70 N4 P V
• Title of publication: Phosphinidene Reactivity of a Transient Vanadium P≡N Complex.
• Authors of publication: Courtemanche, Marc-André; Transue, Wesley J.; Cummins, Christopher C.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 50
• Pages of publication: 16220 - 16223
• a: 10.712 ± 0.007 Å
• b: 10.766 ± 0.006 Å
• c: 20.493 ± 0.012 Å
• α: 93.01 ± 0.011°
• β: 95.875 ± 0.011°
• γ: 111.081 ± 0.01°
• Cell volume: 2183 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.082
• Residual factor for significantly intense reflections: 0.0508
• Weighted residual factors for significantly intense reflections: 0.1213
• Weighted residual factors for all reflections included in the refinement: 0.1369
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No