Information card for entry 4131265

Structure parameters

• Common name: [(Ar*)(3,3-dimethylbutyl)(H/OH)Sn-Sn(Ar*).2toluene Ar* = C6H3-2,6(2,4,6-i-Pr3C6H3)2
• Formula: C92 H127.77 O0.23 Sn2
• Calculated formula: C92 H127.769 O0.2308 Sn2
• Title of publication: Dynamic Behavior and Isomerization Equilibria of Distannenes Synthesized by Tin Hydride/Olefin Insertions: Characterization of the Elusive Monohydrido Bridged Isomer.
• Authors of publication: Wang, Shuai; McCrea-Hendrick, Madison L; Weinstein, Cory M.; Caputo, Christine A.; Hoppe, Elke; Fettinger, James C.; Olmstead, Marilyn M.; Power, Philip P.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 19
• Pages of publication: 6586 - 6595
• a: 11.9437 ± 0.0007 Å
• b: 16.5134 ± 0.001 Å
• c: 20.8121 ± 0.0013 Å
• α: 84.9379 ± 0.0009°
• β: 88.9163 ± 0.0009°
• γ: 88.8673 ± 0.0009°
• Cell volume: 4087.4 ± 0.4 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0631
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.0976
• Weighted residual factors for all reflections included in the refinement: 0.1089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No