Information card for entry 4131348

Structure parameters

• Formula: C36 H51 I O4 Si
• Calculated formula: C36 H51 I O4 Si
• Title of publication: Enantioselective Copper-Catalyzed Oxy-Alkynylation of Diazo Compounds.
• Authors of publication: Hari, Durga Prasad; Waser, Jerome
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 25
• Pages of publication: 8420 - 8423
• a: 9.3812 ± 0.0002 Å
• b: 12.873 ± 0.0002 Å
• c: 29.8093 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3599.9 ± 0.13 ų
• Cell temperature: 140 ± 0.1 K
• Ambient diffraction temperature: 140 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0491
• Weighted residual factors for significantly intense reflections: 0.1364
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No