Information card for entry 4131462

Structure parameters

• Formula: C37 H50 N4 Pd Yb
• Calculated formula: C37 H50 N4 Pd Yb
• Title of publication: Tuning the Stability of Pd(IV) Intermediates Using a Redox Non-innocent Ligand Combined with an Organolanthanide Fragment.
• Authors of publication: Goudy, Violaine; Jaoul, Arnaud; Cordier, Marie; Clavaguéra, Carine; Nocton, Grégory
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 31
• Pages of publication: 10633 - 10636
• a: 9.5134 ± 0.0005 Å
• b: 10.8285 ± 0.0005 Å
• c: 16.8791 ± 0.0009 Å
• α: 103.211 ± 0.002°
• β: 94.076 ± 0.002°
• γ: 93.172 ± 0.002°
• Cell volume: 1683.92 ± 0.15 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0152
• Residual factor for significantly intense reflections: 0.0149
• Weighted residual factors for significantly intense reflections: 0.0401
• Weighted residual factors for all reflections included in the refinement: 0.0403
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No