Information card for entry 4132373

Structure parameters

• Formula: C24 H52 B Cl Li2 O2 Si4
• Calculated formula: C24 H52 B Cl Li2 O2 Si4
• Title of publication: From Borapyramidane to Borole Dianion.
• Authors of publication: Lee, Vladimir Ya; Sugasawa, Haruka; Gapurenko, Olga A.; Minyaev, Ruslan M.; Minkin, Vladimir I.; Gornitzka, Heinz; Sekiguchi, Akira
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 19
• Pages of publication: 6053 - 6056
• a: 9.2197 ± 0.0015 Å
• b: 20.178 ± 0.003 Å
• c: 18.246 ± 0.003 Å
• α: 90°
• β: 103.57 ± 0.002°
• γ: 90°
• Cell volume: 3299.6 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.1173
• Weighted residual factors for all reflections included in the refinement: 0.1259
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No