Information card for entry 4132617

Structure parameters

• Formula: C41 H32 Cl N5 O P2 Ru
• Calculated formula: C41 H32 Cl N5 O P2 Ru
• Title of publication: Insertion of a Nontrigonal Phosphorus Ligand into a Transition Metal-Hydride: Direct Access to a Metallohydrophosphorane.
• Authors of publication: Tanushi, Akira; Radosevich, Alexander T.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 26
• Pages of publication: 8114 - 8118
• a: 11.6372 ± 0.0004 Å
• b: 44.6425 ± 0.0016 Å
• c: 20.0826 ± 0.0007 Å
• α: 90°
• β: 96.7742 ± 0.0011°
• γ: 90°
• Cell volume: 10360.3 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.1143
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No