Information card for entry 4132738

Structure parameters

• Formula: C34 H72 Cl12 N2 Si4
• Calculated formula: C34 H72 Cl12 N2 Si4
• Title of publication: Exhaustively Trichlorosilylated C₁ and C₂ Building Blocks: Beyond the Müller-Rochow Direct Process.
• Authors of publication: Georg, Isabelle; Teichmann, Julian; Bursch, Markus; Tillmann, Jan; Endeward, Burkhard; Bolte, Michael; Lerner, Hans-Wolfram; Grimme, Stefan; Wagner, Matthias
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 30
• Pages of publication: 9696 - 9708
• a: 11.4327 ± 0.0006 Å
• b: 11.8063 ± 0.0006 Å
• c: 19.5139 ± 0.0009 Å
• α: 85.921 ± 0.004°
• β: 85.777 ± 0.004°
• γ: 88.686 ± 0.004°
• Cell volume: 2619.7 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.073
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1414
• Weighted residual factors for all reflections included in the refinement: 0.1476
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No