C-H Bond Addition across a Transient Uranium-Nitrido Moiety and Formation of a Parent Uranium Imido Complex.
Authors of publication
Mullane, Kimberly C.; Ryu, Ho; Cheisson, Thibault; Grant, Lauren N.; Park, Ji Young; Manor, Brian C.; Carroll, Patrick J.; Baik, Mu-Hyun; Mindiola, Daniel J.; Schelter, Eric J.
Journal of publication
Journal of the American Chemical Society
Year of publication
2018
Journal volume
140
Journal issue
36
Pages of publication
11335 - 11340
a
10.9802 ± 0.0005 Å
b
11.5895 ± 0.0005 Å
c
21.4568 ± 0.0009 Å
α
87.954 ± 0.002°
β
87.283 ± 0.002°
γ
65.953 ± 0.002°
Cell volume
2490.31 ± 0.19 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0337
Residual factor for significantly intense reflections
0.0307
Weighted residual factors for significantly intense reflections
0.085
Weighted residual factors for all reflections included in the refinement
0.087
Goodness-of-fit parameter for all reflections included in the refinement
