Information card for entry 4132818

Structure parameters

• Formula: C150 H134 Au10 Cl2 O P8 Pd
• Calculated formula: C150 H134 Au10 Cl2 O P8 Pd
• SMILES: [Au]12345([Au]6789([Au]%10%11%121([Au]1%133([Au]3%144([Au]4%1526([Au]268([Au]87%10([Au]%111([Pd]59%12%13%14%1568[Au]342[P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1)Cl)[P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1)Cl)[P](c1ccccc1)(c1ccccc1)c1ccccc1.O(C(C)C)C(C)C
• Title of publication: Hydride-Mediated Controlled Growth of a Bimetallic (Pd@Au₈)²⁺ Superatom to a Hydride-Doped (HPd@Au₁₀)³⁺ Superatom.
• Authors of publication: Takano, Shinjiro; Hirai, Haru; Muramatsu, Satoru; Tsukuda, Tatsuya
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 39
• Pages of publication: 12314 - 12317
• a: 22.04 ± 0.006 Å
• b: 18.983 ± 0.005 Å
• c: 34.465 ± 0.008 Å
• α: 90°
• β: 97.799 ± 0.004°
• γ: 90°
• Cell volume: 14286 ± 6 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1389
• Weighted residual factors for all reflections included in the refinement: 0.1461
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No