Information card for entry 4133399

Structure parameters

• Formula: C32 H35 Ge O3 P
• Calculated formula: C32 H35 Ge O3 P
• SMILES: [Ge](C(=C\P(=O)(OC(C)C)OC(C)C)\c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Radical Germylzincation of α-Heteroatom-Substituted Alkynes.
• Authors of publication: de la Vega-Hernández, Karen; Romain, Elise; Coffinet, Anais; Bijouard, Kajetan; Gontard, Geoffrey; Chemla, Fabrice; Ferreira, Franck; Jackowski, Olivier; Perez-Luna, Alejandro
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 50
• Pages of publication: 17632 - 17642
• a: 16.3298 ± 0.0009 Å
• b: 12.8553 ± 0.0007 Å
• c: 28.1785 ± 0.0016 Å
• α: 90°
• β: 97.582 ± 0.002°
• γ: 90°
• Cell volume: 5863.6 ± 0.6 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0338
• Residual factor for significantly intense reflections: 0.0273
• Weighted residual factors for significantly intense reflections: 0.0653
• Weighted residual factors for all reflections included in the refinement: 0.0683
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No