Information card for entry 4133405

Structure parameters

• Formula: C27 H63 K Si6 Sn
• Calculated formula: C27 H63 K Si6 Sn
• Title of publication: Mechanochemically Driven Transformations in Organotin Chemistry: Stereochemical Rearrangement, Redox Behavior, and Dispersion-Stabilized Complexes.
• Authors of publication: Koby, Ross F.; Hanusa, Timothy P.; Schley, Nathan D.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 46
• Pages of publication: 15934 - 15942
• a: 12.5863 ± 0.0003 Å
• b: 16.2257 ± 0.0004 Å
• c: 20.9657 ± 0.0006 Å
• α: 90°
• β: 100.864 ± 0.003°
• γ: 90°
• Cell volume: 4204.91 ± 0.19 ų
• Cell temperature: 99.9 ± 0.4 K
• Ambient diffraction temperature: 99.9 ± 0.4 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0678
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for significantly intense reflections: 0.1308
• Weighted residual factors for all reflections included in the refinement: 0.1381
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No