Information card for entry 4133532

Structure parameters

• Formula: C18 H66.5 N8 O35 S6 V5 W
• Calculated formula: C14 H54.5 N7 O39 S7 V5 W
• Title of publication: Self-Assembly of Goldberg Polyhedra from a Concave [WV₅O₁₁(RCO₂)₅(SO₄)]^3- Building Block with 5-Fold Symmetry.
• Authors of publication: Zhang, Yuteng; Gan, Hongmei; Qin, Chao; Wang, Xinlong; Su, Zhongmin; Zaworotko, Michael J.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 50
• Pages of publication: 17365 - 17368
• a: 15.49 ± 0.005 Å
• b: 16.481 ± 0.005 Å
• c: 21.309 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5440 ± 3 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.102
• Weighted residual factors for all reflections included in the refinement: 0.1037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No