Information card for entry 4133537

Structure parameters

• Formula: C540 H240 N60 O324 S10 V60 W12
• Calculated formula: C540 H240 N60 O324 S10 V60 W12
• Title of publication: Self-Assembly of Goldberg Polyhedra from a Concave [WV₅O₁₁(RCO₂)₅(SO₄)]^3- Building Block with 5-Fold Symmetry.
• Authors of publication: Zhang, Yuteng; Gan, Hongmei; Qin, Chao; Wang, Xinlong; Su, Zhongmin; Zaworotko, Michael J.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• Journal volume: 140
• Journal issue: 50
• Pages of publication: 17365 - 17368
• a: 41.893 ± 0.003 Å
• b: 41.893 ± 0.003 Å
• c: 53.783 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 94390 ± 12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.02 K
• Number of distinct elements: 7
• Space group number: 131
• Hermann-Mauguin space group symbol: P 42/m m c
• Hall space group symbol: -P 4c 2
• Residual factor for all reflections: 0.2185
• Residual factor for significantly intense reflections: 0.1385
• Weighted residual factors for significantly intense reflections: 0.3897
• Weighted residual factors for all reflections included in the refinement: 0.4988
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No