Information card for entry 4133630

Structure parameters

• Formula: C55 H67 N5 O2 Si2
• Calculated formula: C55 H67 N5 O2 Si2
• Title of publication: Silicon-Mediated Selective Homo- and Heterocoupling of Carbon Monoxide.
• Authors of publication: Wang, Yuwen; Kostenko, Arseni; Hadlington, Terrance J.; Luecke, Marcel-Philip; Yao, Shenglai; Driess, Matthias
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 1
• Pages of publication: 626 - 634
• a: 16.9921 ± 0.0003 Å
• b: 21.7092 ± 0.0004 Å
• c: 27.5293 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10155.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0762
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.1349
• Weighted residual factors for all reflections included in the refinement: 0.152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No