Crystallography Open Database

Information card for entry 4133655

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Coordinates	4133655.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H106 N4 Re2 Zn2
Calculated formula	C68 H92 N4 Re2 Zn2
Title of publication	Heterotetrametallic Re-Zn-Zn-Re Complex Generated by an Anionic Rhenium(I) β-Diketiminate.
Authors of publication	Lohrey, Trevor D.; Maron, Laurent; Bergman, Robert G.; Arnold, John
Journal of publication	Journal of the American Chemical Society
Year of publication	2019
Journal volume	141
Journal issue	2
Pages of publication	800 - 804
a	12.6151 ± 0.0002 Å
b	12.744 ± 0.0002 Å
c	22.8461 ± 0.0004 Å
α	88.556 ± 0.001°
β	77.634 ± 0.001°
γ	73.542 ± 0.001°
Cell volume	3438.22 ± 0.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0286
Residual factor for significantly intense reflections	0.0218
Weighted residual factors for significantly intense reflections	0.0462
Weighted residual factors for all reflections included in the refinement	0.0486
Goodness-of-fit parameter for all reflections included in the refinement	0.995
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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