Information card for entry 4133681

Structure parameters

• Formula: C32 H79 K O2 Si8
• Calculated formula: C32 H79 K O2 Si8
• Title of publication: Disilene-Silylene Interconversion: A Synthetically Accessible Acyclic Bis(silyl)silylene.
• Authors of publication: Reiter, Dominik; Holzner, Richard; Porzelt, Amelie; Altmann, Philipp J.; Frisch, Philipp; Inoue, Shigeyoshi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 34
• Pages of publication: 13536 - 13546
• a: 14.4278 ± 0.0013 Å
• b: 21.935 ± 0.002 Å
• c: 14.7814 ± 0.0014 Å
• α: 90°
• β: 91.076 ± 0.003°
• γ: 90°
• Cell volume: 4677.1 ± 0.7 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0242
• Weighted residual factors for significantly intense reflections: 0.0552
• Weighted residual factors for all reflections included in the refinement: 0.0575
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No