Information card for entry 4133745

Structure parameters

• Formula: C16 H60 N8 O24 V8
• Calculated formula: C16 H57.564 N8 O24 V8
• Title of publication: LA Dominant Windmill-Shaped V8 Clusters: A Bifunctional Heter-ogeneous Catalyst for CO2 Cycloaddition and Oxidation of Sulfides.
• Authors of publication: Cao, Jia-Peng; Xue, Yun-Shan; Li, Ning-Fang; Gong, Jun-Jie; Kang, Run-Kun; Xu, Yan
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• a: 10.86 ± 0.003 Å
• b: 10.943 ± 0.003 Å
• c: 18.188 ± 0.005 Å
• α: 106.159 ± 0.003°
• β: 98.602 ± 0.003°
• γ: 91.609 ± 0.003°
• Cell volume: 2047.2 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0721
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1666
• Weighted residual factors for all reflections included in the refinement: 0.1717
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No