Information card for entry 4134043

Structure parameters

• Formula: C43 H54 Mo O2 Pb
• Calculated formula: C43 H54 Mo O2 Pb
• Title of publication: Metathetical Exchange between Metal-Metal Triple Bonds.
• Authors of publication: Queen, Joshua D.; Phung, Alice C.; Caputo, Christine A.; Fettinger, James C.; Power, Philip P.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 13.3557 ± 0.0004 Å
• b: 10.6317 ± 0.0003 Å
• c: 28.1313 ± 0.0008 Å
• α: 90°
• β: 94.2515 ± 0.0011°
• γ: 90°
• Cell volume: 3983.5 ± 0.2 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0269
• Weighted residual factors for significantly intense reflections: 0.0512
• Weighted residual factors for all reflections included in the refinement: 0.0549
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No