Information card for entry 4134572

Structure parameters

• Formula: C32 H31 N O8 S
• Calculated formula: C32 H31 N O8 S
• Title of publication: Hydroxylamines as Bifunctional Single-Nitrogen Sources for the Rapid Assembly of Diverse Tricyclic Indole Scaffolds.
• Authors of publication: Fan, Liangxin; Hao, Jiamao; Yu, Jingxun; Ma, Xiaojun; Liu, Jingjing; Luan, Xinjun
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 10.0085 ± 0.0011 Å
• b: 20.427 ± 0.002 Å
• c: 14.7521 ± 0.0016 Å
• α: 90°
• β: 102.161 ± 0.002°
• γ: 90°
• Cell volume: 2948.3 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0744
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.1129
• Weighted residual factors for all reflections included in the refinement: 0.1278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No