Information card for entry 4134752

Structure parameters

• Formula: C33 H59 Cl O3 Si2
• Calculated formula: C33 H59 Cl O3 Si2
• Title of publication: Asymmetric Total Synthesis of (-)-Spirochensilide A.
• Authors of publication: Liang, Xin-Ting; Chen, Jia-Hua; Yang, Zhen
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 10.9749 ± 0.0003 Å
• b: 24.6837 ± 0.0008 Å
• c: 13.5232 ± 0.0004 Å
• α: 90°
• β: 95.884 ± 0.003°
• γ: 90°
• Cell volume: 3644.15 ± 0.19 ų
• Cell temperature: 104.6 K
• Ambient diffraction temperature: 104.6 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0782
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No