Information card for entry 4134823

Structure parameters

• Formula: C84 H154 O24 Si14 U
• Calculated formula: C84 H80 O24 Si14 U
• Title of publication: Uranyl oxo silylation promoted by silsesquioxane coordination.
• Authors of publication: Assefa, Mikiyas K.; Wu, Guang; Hayton, Trevor W.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 18.9919 ± 0.0014 Å
• b: 25.2308 ± 0.0018 Å
• c: 21.8579 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10473.9 ± 1.3 ų
• Cell temperature: 110.04 K
• Ambient diffraction temperature: 110.04 K
• Number of distinct elements: 5
• Space group number: 64
• Hermann-Mauguin space group symbol: C m c e
• Hall space group symbol: -C 2ac 2
• Residual factor for all reflections: 0.0949
• Residual factor for significantly intense reflections: 0.0714
• Weighted residual factors for significantly intense reflections: 0.1784
• Weighted residual factors for all reflections included in the refinement: 0.1936
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No