Information card for entry 4134902

Structure parameters

• Formula: C15 H17 F6 I O2 Si
• Calculated formula: C15 H17 F6 I O2 Si
• Title of publication: Stereoselective Access to Highly Substituted Vinyl Ethers via <i>trans</i>-Difunctionalization of Alkynes with Alcohols and Iodine(III) Electrophile.
• Authors of publication: Ding, Wei; Chai, Jinkui; Wang, Chen; Wu, Junliang; Yoshikai, Naohiko
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 19
• Pages of publication: 8619 - 8624
• a: 7.442 ± 0.0003 Å
• b: 11.8848 ± 0.0005 Å
• c: 12.5542 ± 0.0005 Å
• α: 116.944 ± 0.0013°
• β: 95.0969 ± 0.0014°
• γ: 102.62 ± 0.0015°
• Cell volume: 943.14 ± 0.07 ų
• Cell temperature: 174 ± 2 K
• Ambient diffraction temperature: 174 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0411
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.0512
• Weighted residual factors for all reflections included in the refinement: 0.0556
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No