Information card for entry 4134943

Structure parameters

• Formula: C84 H210 Gd2 K2 N12 O15 Si12
• Calculated formula: C84 H210 Gd2 K2 N12 O15 Si12
• Title of publication: Formation of the End-on Bound Lanthanide Dinitrogen Complexes, [(R2N)3Ln-N=N-Ln(NR2)3]2-, from Divalent [(R2N)3Ln]1- Salts (R = SiMe3).
• Authors of publication: Ryan, Austin J.; Balasubramani, Sreeganesh; Ziller, Joseph W.; Furche, Filipp; Evans, William J.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 15.237 ± 0.003 Å
• b: 20.708 ± 0.005 Å
• c: 21.341 ± 0.005 Å
• α: 75.118 ± 0.003°
• β: 79.221 ± 0.003°
• γ: 76.734 ± 0.003°
• Cell volume: 6275 ± 2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0794
• Weighted residual factors for all reflections included in the refinement: 0.0864
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No