Information card for entry 4135321

Structure parameters

• Formula: C72 H152 N2 O17 Si4 U
• Calculated formula: C72 H152 N2 O17 Si4 U
• Title of publication: Photochemical Synthesis of a Stable Terminal Uranium(VI) Nitride
• Authors of publication: Barluzzi, Luciano; Scopelliti, Rosario; Mazzanti, Marinella
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 13.8047 ± 0.0002 Å
• b: 18.2614 ± 0.0004 Å
• c: 18.3619 ± 0.0004 Å
• α: 91.9047 ± 0.0017°
• β: 91.0275 ± 0.0016°
• γ: 101.261 ± 0.0016°
• Cell volume: 4535.87 ± 0.16 ų
• Cell temperature: 140 ± 0.1 K
• Ambient diffraction temperature: 140 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0575
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0793
• Weighted residual factors for all reflections included in the refinement: 0.089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No