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Information card for entry 4135361
Preview
Coordinates | 4135361.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C184 H204 Cl24 N4 O32 Rh8 |
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Calculated formula | C184 H204 Cl24 N4 O32 Rh8 |
Title of publication | <i>In Crystallo</i> Snapshots of Rh<sub>2</sub>-Catalyzed C-H Amination. |
Authors of publication | Das, Anuvab; Wang, Chen-Hao; Van Trieste, 3rd, Gerard P; Sun, Cheng-Jun; Chen, Yu-Sheng; Reibenspies, Joseph H.; Powers, David C. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2020 |
Journal volume | 142 |
Journal issue | 47 |
Pages of publication | 19862 - 19867 |
a | 15.6237 ± 0.0009 Å |
b | 17.2551 ± 0.0008 Å |
c | 19.6274 ± 0.0013 Å |
α | 111.577 ± 0.002° |
β | 94.521 ± 0.002° |
γ | 96.215 ± 0.002° |
Cell volume | 4851.2 ± 0.5 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0465 |
Residual factor for significantly intense reflections | 0.0386 |
Weighted residual factors for significantly intense reflections | 0.0819 |
Weighted residual factors for all reflections included in the refinement | 0.0854 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.101 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4135361.html
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