Information card for entry 4135364

Structure parameters

• Formula: C20 H26 N O2 P
• Calculated formula: C20 H26 N O2 P
• Title of publication: Copper(I)-Catalyzed Asymmetric 1,4-Conjugate Hydrophosphination of α,β-Unsaturated Amides.
• Authors of publication: Li, Yan-Bo; Tian, Hu; Yin, Liang
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 47
• Pages of publication: 20098 - 20106
• a: 7.9196 ± 0.0003 Å
• b: 8.505 ± 0.0004 Å
• c: 27.304 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1839.09 ± 0.14 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 169.99 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No