Information card for entry 4135378

Structure parameters

• Formula: C18 H21 B F N
• Calculated formula: C18 H21 B F N
• Title of publication: Insertion of Alkylidene Carbenes into B-H Bonds.
• Authors of publication: Yang, Ji-Min; Guo, Feng-Kai; Zhao, Yu-Tao; Zhang, Qiao; Huang, Ming-Yao; Li, Mao-Lin; Zhu, Shou-Fei; Zhou, Qi-Lin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 11.84648 ± 0.00007 Å
• b: 6.18222 ± 0.00005 Å
• c: 21.5257 ± 0.00012 Å
• α: 90°
• β: 90.2727 ± 0.0005°
• γ: 90°
• Cell volume: 1576.47 ± 0.018 ų
• Cell temperature: 294.15 K
• Ambient diffraction temperature: 294.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0434
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for significantly intense reflections: 0.1148
• Weighted residual factors for all reflections included in the refinement: 0.1167
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No