Information card for entry 4135390

Structure parameters

• Formula: C33.75 H36 Cl N2 Ni P2
• Calculated formula: C33.75 H36 Cl N2 Ni P2
• Title of publication: Enthalpy-Controlled Insertion of a "Nonspectator" Tricoordinate Phosphorus Ligand into Group 10 Transition Metal-Carbon Bonds.
• Authors of publication: Hwang, Seung Jun; Tanushi, Akira; Radosevich, Alexander T.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 51
• Pages of publication: 21285 - 21291
• a: 15.4791 ± 0.0013 Å
• b: 15.4791 ± 0.0013 Å
• c: 26.403 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6326.2 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 99.99 K
• Number of distinct elements: 6
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0611
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.1476
• Weighted residual factors for all reflections included in the refinement: 0.1547
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No