Information card for entry 4135395

Structure parameters

• Formula: C162 H257 B3 Si9
• Calculated formula: C162 H257 B3 Si9
• Title of publication: A Neutral Silicon(II) Half-Sandwich Compound.
• Authors of publication: Heitkemper, Tobias; Sarcevic, Julijan; Sindlinger, Christian P.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 51
• Pages of publication: 21304 - 21309
• a: 11.5159 ± 0.0014 Å
• b: 26.624 ± 0.003 Å
• c: 28.024 ± 0.003 Å
• α: 75.516 ± 0.002°
• β: 86.674 ± 0.002°
• γ: 89.643 ± 0.002°
• Cell volume: 8304.7 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1314
• Residual factor for significantly intense reflections: 0.0946
• Weighted residual factors for significantly intense reflections: 0.2433
• Weighted residual factors for all reflections included in the refinement: 0.27
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No