Information card for entry 4300055

Structure parameters

• Formula: C28 H31 Cl2 F6 N2 P2 Rh
• Calculated formula: C28 H31 Cl2 F6 N2 P2 Rh
• Title of publication: Rhodium Complexes with the Chelating and Binucleating Ligands P(CH~2~CH~2~Py)~n~Ph~3-n~, (Py = 2-Pyridyl; n= 1, 2): Structures and Fluxional Behavior
• Authors of publication: M. Aránzazu Alonso; Juan A. Casares; Pablo Espinet; Katerina Soulantica; Jonathan P. H. Charmant; A. Guy Orpen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 705 - 711
• a: 8.4552 ± 0.001 Å
• b: 18.0676 ± 0.0032 Å
• c: 19.7286 ± 0.0027 Å
• α: 90°
• β: 99.658 ± 0.007°
• γ: 90°
• Cell volume: 2971.1 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0382
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for all reflections: 0.066
• Weighted residual factors for significantly intense reflections: 0.0624
• Goodness-of-fit parameter for all reflections: 0.998
• Goodness-of-fit parameter for significantly intense reflections: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No