Information card for entry 4300085

Structure parameters

• Formula: C16 H48 Ag3 La O8 S8 Se12 W3
• Calculated formula: C16 H48 Ag3 La O8 S8 Se12 W3
• Title of publication: Heterometallic Polymeric Clusters Containing Tetraselenotungstate Anion: One-Dimensional Helical Chain {[La(Me2SO)8][(μ-WSe4)3Ag3]}n and Cyanide-Bridged Three-Dimensional Cross-Framework {[Et4N]2[(μ4-WSe4)Cu4(CN)4]}n
• Authors of publication: Qian-Feng Zhang; Wa-Hung Leung; Xin; Hoong-Kun Fun
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 417 - 426
• a: 12.7642 ± 0.0005 Å
• b: 24.1725 ± 0.0009 Å
• c: 19.4012 ± 0.0007 Å
• α: 90°
• β: 103.564 ± 0.001°
• γ: 90°
• Cell volume: 5819.1 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1251
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1116
• Weighted residual factors for all reflections included in the refinement: 0.136
• Goodness-of-fit parameter for all reflections included in the refinement: 0.945
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No