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Information card for entry 4301295
Preview
Coordinates | 4301295.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C76 H158 Na2 O22 P4 Si2 |
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Calculated formula | C76 H158 Na2 O22 P4 Si2 |
SMILES | C(C)(C)(C)[Si](C(C)(C)C)(C(C)(C)C)P=PP=P[Si](C(C)(C)C)(C(C)(C)C)C(C)(C)C.[Na]12345([O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)([O]1CCCC1)[O]1CCCC1.[Na]12345([O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)([O]1CCCC1)[O]1CCCC1.C1COCCOCCOCCOCCOCCO1 |
Title of publication | Supersilylated Tetraphosphene Derivatives M2[t-Bu3SiPPPPSi-t-Bu3] (M = Li, Na, Rb, Cs) and Ba[t-Bu3SiPPPPSi-t-Bu3]: Reactivity and Cis-Trans Isomerization |
Authors of publication | Andreas Lorbach; Andor Nadj; Sandor Tüllmann; Franz Dornhaus; Frauke Schödel; Inge Sänger; Günter Margraf; Jan W. Bats; Michael Bolte; Max C. Holthausen; Matthias Wagner; Hans-Wolfram Lerner |
Journal of publication | Inorganic Chemistry |
Year of publication | 2009 |
Journal volume | 48 |
Pages of publication | 1005 - 1017 |
a | 16.006 ± 0.002 Å |
b | 23.823 ± 0.003 Å |
c | 16.436 ± 0.002 Å |
α | 90° |
β | 115.699 ± 0.01° |
γ | 90° |
Cell volume | 5647.3 ± 1.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.3635 |
Residual factor for significantly intense reflections | 0.2468 |
Weighted residual factors for significantly intense reflections | 0.5331 |
Weighted residual factors for all reflections included in the refinement | 0.5762 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.361 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4301295.html
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