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Information card for entry 4301318
Preview
Coordinates | 4301318.cif |
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Original paper (by DOI) | HTML |
Formula | C26 H26 Cl6 N2 Ni O5 |
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Calculated formula | C26 H26 Cl6 N2 Ni O5 |
SMILES | [Ni]123[N](c4c([N]2=Cc2c(O1)c(OCC)ccc2)cccc4)=Cc1cccc(OCC)c1O3.ClC(Cl)Cl.ClC(Cl)Cl.O |
Title of publication | Isolation and Structural Characterization of a Binuclear Intermediate Species Pertinent to Transmetalation of Zn(salphen) Complexes and the Formation of Polynuclear Salen Structures |
Authors of publication | Leire San Felices; Eduardo C. Escudero-Adán; Jordi Benet-Buchholz; Arjan W. Kleij |
Journal of publication | Inorganic Chemistry |
Year of publication | 2009 |
Journal volume | 48 |
Pages of publication | 846 - 853 |
a | 9.2322 ± 0.0002 Å |
b | 11.6101 ± 0.0003 Å |
c | 14.4864 ± 0.0004 Å |
α | 90.748 ± 0.001° |
β | 95.533 ± 0.001° |
γ | 107.258 ± 0.001° |
Cell volume | 1474.52 ± 0.06 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0347 |
Residual factor for significantly intense reflections | 0.0306 |
Weighted residual factors for significantly intense reflections | 0.0828 |
Weighted residual factors for all reflections included in the refinement | 0.0856 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4301318.html
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Users of the data should acknowledge the original authors of the
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