Information card for entry 4301346

Structure parameters

• Formula: C29 H43 Ge N3
• Calculated formula: C29 H43 Ge N3
• SMILES: [Ge]1([N](c2c(C(C)C)cccc2C(C)C)=C(C=C(C)N1c1c(C(C)C)cccc1C(C)C)C)N
• Title of publication: Cleavage of a N-H Bond of Ammonia at Room Temperature by a Germylene
• Authors of publication: Anukul Jana; Ina Objartel; Herbert W. Roesky; Dietmar Stalke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 798 - 800
• a: 24.902 ± 0.005 Å
• b: 15.167 ± 0.003 Å
• c: 14.672 ± 0.003 Å
• α: 90°
• β: 95.261 ± 0.003°
• γ: 90°
• Cell volume: 5518.1 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.1005
• Weighted residual factors for all reflections included in the refinement: 0.1048
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No