Information card for entry 4301633

Structure parameters

• Formula: C53 H58 N Ni O1.5 P S
• Calculated formula: C53 H58 N Ni O1.5 P S
• Title of publication: Synthesis and Reactions of Mono- and Dinuclear Ni(I) Thiolate Complexes
• Authors of publication: Mikinao Ito; Tsuyoshi Matsumoto; Kazuyuki Tatsumi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 2215 - 2223
• a: 39.992 ± 0.01 Å
• b: 12.637 ± 0.003 Å
• c: 19.189 ± 0.005 Å
• α: 90°
• β: 100.963 ± 0.003°
• γ: 90°
• Cell volume: 9521 ± 4 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0633
• Weighted residual factors for all reflections included in the refinement: 0.1818
• Goodness-of-fit parameter for all reflections included in the refinement: 1.183
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No