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Information card for entry 4301677
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Coordinates | 4301677.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [SiPiPr3]Ir(H)(Cl) |
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Formula | C42 H61 Cl Ir P3 Si |
Calculated formula | C42 H60 Cl Ir P3 Si |
SMILES | [Ir]123([Si](c4ccccc4[P]1(C(C)C)C(C)C)(c1ccccc1[P]2(C(C)C)C(C)C)c1ccccc1[P]3(C(C)C)C(C)C)Cl.c1ccccc1 |
Title of publication | Dinitrogen Complexes Supported by Tris(phosphino)silyl Ligands |
Authors of publication | Matthew T. Whited; Neal P. Mankad; Yunho Lee; Paul F. Oblad; Jonas C. Peters |
Journal of publication | Inorganic Chemistry |
Year of publication | 2009 |
Journal volume | 48 |
Pages of publication | 2507 - 2517 |
a | 19.5771 ± 0.0015 Å |
b | 11.0445 ± 0.0009 Å |
c | 18.5937 ± 0.0014 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4020.3 ± 0.5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.0538 |
Residual factor for significantly intense reflections | 0.0394 |
Weighted residual factors for significantly intense reflections | 0.0802 |
Weighted residual factors for all reflections included in the refinement | 0.0857 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.077 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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