Crystallography Open Database

Information card for entry 4301966

4301965 << 4301966 >> 4301967

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Coordinates	4301966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H45 F6 N2 P3 Pd
Calculated formula	C21 H45 F5.998 N2 P3 Pd
Title of publication	Palladium N(CH2CH2PiPr2)2-Dialkylamides: Synthesis, Structural Characterization, and Reactivity
Authors of publication	Alexander N. Marziale; Eberhardt Herdtweck; Jörg Eppinger; Sven Schneider
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	3699 - 3709
a	9.5853 ± 0.0001 Å
b	15.7998 ± 0.0002 Å
c	19.5797 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	2965.26 ± 0.06 Å³
Cell temperature	153 ± 1 K
Ambient diffraction temperature	153 ± 1 K
Number of distinct elements	6
Space group number	57
Hermann-Mauguin space group symbol	P b c m
Hall space group symbol	-P 2c 2b
Residual factor for all reflections	0.0419
Residual factor for significantly intense reflections	0.0353
Weighted residual factors for significantly intense reflections	0.0782
Weighted residual factors for all reflections included in the refinement	0.0828
Goodness-of-fit parameter for all reflections included in the refinement	1.158
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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