Information card for entry 4302033

Structure parameters

• Formula: C65 H90 Ga N4 O2 P2 Si2 Y
• Calculated formula: C65 H90 Ga N4 O2 P2 Si2 Y
• Title of publication: A Heterobimetallic Gallyl Complex Containing an Unsupported Ga-Y Bond
• Authors of publication: Stephen T. Liddle; David P. Mills; Benedict M. Gardner; Jonathan McMaster; Cameron Jones; William D. Woodul
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 3520 - 3522
• a: 13.4466 ± 0.0008 Å
• b: 21.0498 ± 0.0012 Å
• c: 23.1044 ± 0.0013 Å
• α: 90°
• β: 94.113 ± 0.002°
• γ: 90°
• Cell volume: 6522.8 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0668
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.0851
• Weighted residual factors for all reflections included in the refinement: 0.0956
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No