Information card for entry 4302403

Structure parameters

• Formula: C173 H150 F24 Lu2 N36 O27 S8 Zn
• Calculated formula: C170 H150 F15 Lu2 N36 O18 S5 Zn
• Title of publication: Self-Assembly of the First Discrete 3d‒4f‒4f Triple-Stranded Helicate
• Authors of publication: Riis-Johannessen, Thomas; Bernardinelli, Gérald; Filinchuk, Yaroslav; Clifford, Sarah; Dalla Favera, Natalia; Piguet, Claude
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Journal issue: 12
• Pages of publication: 5512 - 5525
• a: 15.8708 ± 0.0008 Å
• b: 16.0222 ± 0.0005 Å
• c: 47.308 ± 0.002 Å
• α: 90.679 ± 0.004°
• β: 93.321 ± 0.004°
• γ: 117.501 ± 0.004°
• Cell volume: 10642.4 ± 0.9 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1779
• Residual factor for significantly intense reflections: 0.1517
• Weighted residual factors for significantly intense reflections: 0.4149
• Weighted residual factors for all reflections included in the refinement: 0.4495
• Goodness-of-fit parameter for all reflections included in the refinement: 1.721
• Diffraction radiation wavelength: 0.72242 Å
• Diffraction radiation type: synchrotron
• Duplicate of: 4338553
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No