Information card for entry 4302431

Structure parameters

• Formula: C45.5 H62.5 N15.5 Ni O9.5 Tb W
• Calculated formula: C45.5 H62.5 N15.5 Ni O9.5 Tb W
• Title of publication: Hetero-Metallic {3d-4f-5d} Complexes: Preparation and Magnetic Behavior of Trinuclear [(LMe2Ni-Ln){W(CN)8}] Compounds (Ln = Gd, Tb, Dy, Ho, Er, Y; LMe2= Schiff base) and Variable SMM Characteristics for the Tb Derivative
• Authors of publication: Jean-Pascal Sutter; Sébastien Dhers; Jean-Pierre Costes; Carine Duhayon; Laure Vendier; Raghunathan Rajamani; S. Ramasesha
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 5820 - 5828
• a: 11.9038 ± 0.001 Å
• b: 25.841 ± 0.002 Å
• c: 19.8029 ± 0.0015 Å
• α: 90°
• β: 106.362 ± 0.002°
• γ: 90°
• Cell volume: 5844.8 ± 0.8 ų
• Cell temperature: 180 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for all reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.0335
• Weighted residual factors for all reflections included in the refinement: 0.0321
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No