Information card for entry 4302657

Structure parameters

• Formula: C48 H108 Cl9 Cu8 N8 Na5 O114 Sm4
• Calculated formula: C48 H108 Cl9 Cu8 N8 Na5 O114 Sm4
• Title of publication: From Metalloligand to Interpenetrating Channels: Synthesis, Characterization, and Properties of a 2p-3d-4f Heterometallic Coordination Polymer {[Na5Cu8Sm4(NTA)8(ClO4)8(H2O)22].ClO4.8H2O}n
• Authors of publication: Jing-xin Ma; Xiao-feng Huang; You Song; Xue-qin Song; Wei-sheng Liu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 6326 - 6328
• a: 17.041 ± 0.0014 Å
• b: 17.041 ± 0.0014 Å
• c: 25.371 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7367.6 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0538
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.1234
• Weighted residual factors for all reflections included in the refinement: 0.1302
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No