Information card for entry 4302865

Structure parameters

• Chemical name: 1-azido-2,4-bis[2,4-bis-(2,4,6-trimethylphenyl)phenyl]-cyclo-1,3-diarsa -2,4-diazenium bis[hexachloridogallate(III)] 1-chloro-2,4-bis[2,4-bis-(2,4,6-trimethylphenyl)phenyl]-cyclo-1,3-diarsa -2,4-diazenium bis[hexachloridogallate(III)]
• Formula: C48 H50 As2 Cl6.75 Ga2 N5.75
• Calculated formula: C48 H50 As2 Cl6.75 Ga2 N5.75
• Title of publication: Cyclic Arsenic-Nitrogen Cations
• Authors of publication: Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 7359 - 7367
• a: 16.066 ± 0.002 Å
• b: 15.044 ± 0.003 Å
• c: 22.265 ± 0.004 Å
• α: 90°
• β: 104.361 ± 0.011°
• γ: 90°
• Cell volume: 5213.2 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0326
• Residual factor for significantly intense reflections: 0.0238
• Weighted residual factors for significantly intense reflections: 0.0541
• Weighted residual factors for all reflections included in the refinement: 0.0572
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No