Information card for entry 4303436

Structure parameters

• Formula: C145 H132 Cu4 N24
• Calculated formula: C145 H132 Cu4 N24
• Title of publication: Oligonuclear Homoleptic Copper(I) Pyrazolates with Multinucleating Ligand Scaffolds: High Structural Diversity in Solid-State and Solution
• Authors of publication: Michael Stollenz; Michael John; Henrike Gehring; Sebastian Dechert; Christian Grosse; Franc Meyer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 10049 - 10059
• a: 15.7778 ± 0.0005 Å
• b: 18.3074 ± 0.0007 Å
• c: 24.0587 ± 0.0008 Å
• α: 104.105 ± 0.002°
• β: 93.087 ± 0.002°
• γ: 115.284 ± 0.002°
• Cell volume: 5994.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0901
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1473
• Weighted residual factors for all reflections included in the refinement: 0.1683
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No