Information card for entry 4303990

Structure parameters

• Formula: C75 H112 P4 Sn2
• Calculated formula: C75 H104 P4 Sn2
• Title of publication: Unusual Reactivity of Methylphosphaalkyne (P\τbCMe) toward Digermenes and Distannenes: Stepwise Formations of Bridged 2,3,5,6-Tetraphospha-1,4-dimethylidenecyclohexanes
• Authors of publication: Cameron Jones; Christian Schulten; Andreas Stasch
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1273 - 1278
• a: 10.727 ± 0.002 Å
• b: 12.633 ± 0.003 Å
• c: 14.198 ± 0.003 Å
• α: 71.7 ± 0.03°
• β: 80.66 ± 0.03°
• γ: 83.61 ± 0.03°
• Cell volume: 1798.8 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0361
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0698
• Weighted residual factors for all reflections included in the refinement: 0.0723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No