Information card for entry 4304205

Structure parameters

• Formula: C22 H51 Br N2 Ni P2 Si
• Calculated formula: C22 H47 Br N2 Ni P2 Si
• Title of publication: First-Row Transition Metal-Halide Complexes Supported by a Monoanionic [N2P2] Ligand
• Authors of publication: Wayne A. Chomitz; Seth F. Mickenberg; John Arnold
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 373 - 380
• a: 16.555 ± 0.003 Å
• b: 11.593 ± 0.002 Å
• c: 14.908 ± 0.003 Å
• α: 90°
• β: 92.564 ± 0.003°
• γ: 90°
• Cell volume: 2858.3 ± 0.9 ų
• Cell temperature: 156 ± 2 K
• Ambient diffraction temperature: 156 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0815
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.1001
• Weighted residual factors for all reflections included in the refinement: 0.1076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.175
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No