Information card for entry 4304359

Structure parameters

• Formula: C23 H52 N Ni O2 P2 Si2
• Calculated formula: C23 H52 N Ni O2 P2 Si2
• Title of publication: O/C Bond Cleavage of CO2 by NiI
• Authors of publication: Benjamin C. Fullmer; Hongjun Fan; Maren Pink; Kenneth G. Caulton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1865 - 1867
• a: 11.386 ± 0.002 Å
• b: 14.891 ± 0.003 Å
• c: 18.133 ± 0.003 Å
• α: 90°
• β: 100.413 ± 0.004°
• γ: 90°
• Cell volume: 3023.8 ± 1 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0308
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0623
• Weighted residual factors for all reflections included in the refinement: 0.0663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No