Information card for entry 4304420

Structure parameters

• Formula: C19 H22 Cl2 N O0.5 Re
• Calculated formula: C19 H22 Cl2 N O0.5 Re
• Title of publication: Oxygen-Centered Hexatantalum Tetradecaimido Cluster Complexes
• Authors of publication: Jamin L. Krinsky; Laura L. Anderson; John Arnold; Robert G. Bergman
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1053 - 1066
• a: 8.4832 ± 0.0015 Å
• b: 17.131 ± 0.003 Å
• c: 13.904 ± 0.002 Å
• α: 90°
• β: 102.723 ± 0.002°
• γ: 90°
• Cell volume: 1971 ± 0.6 ų
• Cell temperature: 157 ± 2 K
• Ambient diffraction temperature: 157 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0403
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0544
• Weighted residual factors for all reflections included in the refinement: 0.0575
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No