Crystallography Open Database

Information card for entry 4304554

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Coordinates	4304554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Al13 H90 N15 O102
Calculated formula	Al13 H72.02 N6 O68
Title of publication	Facile Synthesis of the Tridecameric Al13 Nanocluster Al13(μ3-OH)6(μ2-OH)18(H2O)24(NO3)15
Authors of publication	Jason T. Gatlin; Zachary L. Mensinger; Lev N. Zakharov; David MacInnes; Darren W. Johnson
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	1267 - 1269
a	12.8256 ± 0.0008 Å
b	13.1667 ± 0.0008 Å
c	13.4201 ± 0.0008 Å
α	77.601 ± 0.001°
β	74.059 ± 0.001°
γ	87.648 ± 0.001°
Cell volume	2127.9 ± 0.2 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0571
Residual factor for significantly intense reflections	0.0479
Weighted residual factors for significantly intense reflections	0.1264
Weighted residual factors for all reflections included in the refinement	0.1322
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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